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1、-附表附表 1 1 页岩油性质页岩油性质项目样品名称密度20粘度20粘度50凝固点闪点闭口氯盐酸值残炭灰分胶质沥青质碱性氮含量硫铁镍钙钠钒水分计量单位kg/m3mm2/smm2/smgNaClLmgKOH/g%(m/m)%(m/m)%m/m%m/m%m/m%m/mg/gg/gg/gg/gg/g%m/m检测结果*宝明2014-1-90.8900-910014.825.34810682.70.521.60.01615.730.290.58680.3206.340.4632.521.590.0290.5分析方法SH/T 0604-2000GB/T 11137-1989GB/T 11137-1989G
2、B/T 510-1991GB/T261-91SY/T 0536-2021GB/T 264-1991SH/T0170-2000GB/T 508-1991Q/SY WH Yj 0716-2021Q/SY WH Yj 0716-2021ASTM D 5762-2021GB/T17606-2021Q/SY WH Yj 0742-2021Q/SY WH Yj 0742-2021Q/SY WH Yj 0742-2021Q/SY WH Yj 0742-2021Q/SY WH Yj 0742-2021GB/T8929-2006金属含量附表附表 2 2 页岩油恩氏馏程收率页岩油恩氏馏程收率工程样品名称恩氏馏程：
3、初馏点100120140160180200220240260280300全馏量计量单位%V/V%V/V%V/V%V/V%V/V%V/V%V/V%V/V%V/V%V/V%V/V%V/V检测结果*17200000.52.07.515.525.032.540.042.0分析方法GB/T255-1988GB/T255-1998GB/T255-1998GB/T255-1998GB/T255-1998GB/T255-1998GB/T255-1998GB/T255-1998GB/T255-1998GB/T255-1998GB/T255-1998GB/T255-1998GB/T255-1998.z.-附表附表
4、 3 3 页岩油实沸点蒸馏收率页岩油实沸点蒸馏收率样品名称项目馏程：初馏点IBP-100120140160180200220240260280300320340360380400420440460480500页岩油计量单位%m/m%m/m%m/m%m/m%m/m%m/m%m/m%m/m%m/m%m/m%m/m%m/m%m/m%m/m%m/m%m/m%m/m%m/m%m/m%m/m%m/m单计收率0.980.980.090.090.070.070.180.180.750.755.225.221.551.552.572.573.703.705.295.299.509.509.709.707.047
5、.046.606.607.907.905.635.635.595.595.675.674.304.303.253.253.703.70采样时间2014-02-6分析方法检测结果累计收率0.980.981.061.061.131.131.311.312.062.067.287.288.838.8311.4011.4015.1015.1020.3920.3929.8929.8939.5939.5946.6346.6353.2353.2361.1361.1366.7666.7672.3572.3578.0278.0282.3282.3285.5785.5789.2789.27GB/T18211200
6、1.z.-附表附表 4 4 页岩油窄馏分性质页岩油窄馏分性质沸程收率，w%单计IBP-100100-120120-140140-160160-180180-200200-220220-240240-260260-280280-300300-320320-340340-360360-380380-400400-420420-440440-460460-480480-500500累计密度g/cm30.70950.20920.75070.76960.78060.79920.82010.83150.83900.84660.85860.86170.87930.8819酸度/值mgKOH/100mmgKO
7、H/gl0.621.354.6510.1510.238.400.300.550.560.600.370.460.38硫含量mg/kg129160182182176177189252293327390401496565氮含量mg/kg300306336695907995折光率 20200.9621.1951.3992.0372.6503.1954.7775.8088.62313.26粘度,mm2/s50100/1.0401.3121.6262.0173.2214.065凝固点/-47-38-35-27-23-17-514苯胺点/32.033.535.037.540.041.042.044.650
8、.051.00.980.090.070.180.755.221.552.573.705.299.509.707.046.607.905.635.595.674.303.253.7010.680.981.061.131.312.067.288.8311.4015.1020.3929.8939.5946.6353.2361.1366.7672.3578.0282.3285.5789.2799.95.z.-附表附表 5 5 页岩油重整原料及石脑性质页岩油重整原料及石脑性质项目沸点范围收率密度20总氮硫含量砷酸度硫醇硫溴价铜片腐蚀总烷烃总环烷烃总芳香烃芳烃潜含量计量单位mkg/m3g/gg/gng/g
9、mgKOH100m1%(m/m)gBr/100g(级)%m/m%m/m%m/m%m/m参考指标3.0400200检测结果初馏1601.31738.0325299563.37.70.31b31.836.5015.2419.48检测结果初馏2007.28757.1556399557.28.20.41b33.928.2414.6711.45分析方法GB/T172802021GB/T172802021SH/T 0604-2000ASTM D 4629-2021SH/T 0689-2000Q/SY WH Yj 0709-2021GB/T 258-1977(2004)GB/T 1792-1988SH/T
10、0630-1996(2004)GB/T5096-1985(2004)STM D 6839-2002(2007)STM D 6839-2002(2007)STM D 6839-2002(2007)原油评价方法附表附表 6 6 页岩油航空喷气燃料馏分性质页岩油航空喷气燃料馏分性质项目沸点范围收率密度20粘度(20)酸度硫含量硫醇硫铜片腐蚀冰点闪点闭口饱和烃芳烃烯烃萘系烃碘值馏程：初馏点10蒸发温度30蒸发温度50蒸发温度70蒸发温度90蒸发温度95蒸发温度终馏点计量单位mkg/m3mm2/smgKOH100m1g/g%m/m(级)%v/v%v/v%v/v%m/mgI/100g参考指标3#航煤1.2
11、51.020000.0021-4738-20-204232-280检测结果120-26014.04852.43.6121.0126600.0031b-4742.590.09.30.74.750.95116.2148.1168.7188.1208.1230.0246.7247.8分析方法GB/T172801998GB/T172801998SH/T0604-2000GB/T265-1988GB/T 258-1977(2004)SH/T 0689-2000GB/T1792-1988GB/T5096-1985(2004)GB/T2430-2021GB/T261-2021GB/T11132-2021GB
12、/T11132-2021GB/T11132-2021SH/T0181-2005SH/T0234-19922004GB/T6536-2021GB/T6536-2021GB/T6536-2021GB/T6536-2021GB/T6536-2021GB/T6536-2021GB/T6536-2021GB/T6536-2021附表附表 7 7 页岩油柴油馏分性质页岩油柴油馏分性质项目沸点范围计量单位参考指标200-260检测结果200-360260-360.z.-收率密度20粘度(20)酸度水分硫含量铜片腐蚀50，3h凝点冷滤点苯胺点闭口闪点十六烷值十六烷指数馏程：初馏点10回收温度30回收温度50回
13、收温度70回收温度90回收温度95回收温度终馏点回收百分数残留物百分数总损失百分数mkg/m3mm2/smgKOH100m1g/g(级)%v/v%v/v%v/v7.0500110、5、0、-10-20、-35、-50-4551-300-355-7.82862.72.6127.25901b低于-35-3541.0664042187.0200.4209.7218.1226.7239.1248.5257.998.01.80.245.95871.76.9569.5痕迹27301b-19-1046.3954446198.0230.0251.0271.0294.0322.0331.635098.01.80
14、.238.13874.412.72119.5痕迹25601b-16-648.91324648222.0235.0251.0275.0299.0327.0347.0356.098.51.30.2附表附表 8 8 页岩油页岩油 VGOVGO 性质性质项目沸点范围收率密度20粘度(50)粘度(100)酸值凝固点残炭灰分饱和烃芳烃胶质沥青质分子量元素分析金属碳氢硫氮铁镍计量单位mkg/m3mm2/smm2/smgKOH/g%(m/m)%(m/m)%(m/m)%(m/m)%(m/m)%(m/m)%m/m%m/m%m/m%m/mg/gg/g乌石化参考指标加氢裂化360-5000.20.21.52.0.z.催化裂化360-5000.090.1检测结果360-50036.04925.159.958.7220.83270.50.00161.227.511.350010.68987.59403360.693319.890.2698588.279.360.3860.5099.77.3826.667.10.3410.6410.2753.3455.627.112.25.1.z.