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1、皮勒数 (10-6)花岗岩 GBW07103(GSR-1)安山岩 GBW07104(GSR-2)玄武岩GBW07105 (GSR-3)石英砂岩 GBW07106 (GSR-4)页岩GBW07107 (GSR-5)泥质灰岩 GBW07108 (GSR-6)石灰岩 GBW07120 (GSR-13)才幽片麻岩 GBW07121 (GSR-14)斜做幅 GBW07122 (GSR-15)Ag0.033 0.0070.071 0.0090.040 0.0080.062 0.0070.047 0.0090.043 0.011(0.025)0.03 0.01(0.05)As2.1 0.42.1 0.4(0
2、.7)9.1 + 1.21.4 0.34.70.60.66 0.11(0.25)263Au(0,00055)(0.00095)(0.00066)(0.0018)(0.0010)(0,00094)B24 + 34.7+0.83.5+1.034 + 6154+11164(12)153122Ba343 29102() 455272614314450 2912()12921140 8()6214BeI2.41.4l.l0.22.50.40.970.103.00.30.80.20.14 0.031.70.30.340.06BiO.53O.O6a08l 0.0160.048 0.0170.18 0.030
3、.230.030.160.040.032 0.0070.096 0.016(0.06)Br(0.4)(0.3)Cd0.029 + 0.0090.061+0.0140.067+0.0160.060 + 0.0160.033+0.0120.07+0.020.016+0.006(0.06)(0. 14)Ce108740 3l()584841(982534.6 0.44837.7 1.()ClI2717(46)(114)(44)4167815(24)(120)(116)Co3.4 0.7I3.21.O46.53.46.4 0.621+2920.80.37.8+1.1525Cr3.6 + 0.9323I
4、34ll20 + 39963263.4 0.42421375Cs38.4 1.22.3+0.7(0.7)1.80.31423.2+0.7(0. 10)2.6+0.31.8 + 0.3Cu3.2 0.955349319242 22322.2 0.3(3. 1)845Dy10.2 0.41.85+0.175.6 + 034.1 0.45.1 0.41.6 0.20.280.071.520.143.5 0.5Er6.50.3O.85O.I32.00.22.0 0.32.70.41.00.2(0. 17)0.760.082.3 0.4Eu0.85 0.071.02 0.053.2 0.21.02 0.
5、081.7 0.2().51 0.05().082 0.0191.0 0.2().91 0.15F2350+128280 25700 + 44183+181290+64406 + 29249+18670 + 84200 + 20Ga19218.11.424.8 0.95.3 0.82637.1 0.80.87 0.1718.21.617.2 1.0Gd9.30.72.70.48.50.64.50.46.70.51.9 0.20.360.082.40.32.80.3Gc2.00.3O.93O.I50.980.2l1.160.273.1 0.50.670.200.14 0.030.93 0.071
6、.46 0.20Hf63 0.82.9 0.56.5 0.86.6 0.72.9 0.51.8 0.30.22 0.053.3 0.51.5 0.2HgO.OMl土0.012+0.0030.006 + 0.0020.008 + 0.0020.010+0.0020.016+0.0020.005 + 0.0020.0035 + 0.00160.0033+().(X)I2().(XX)8Ho2.050.170.34 0.03O.88O.O40.750.120.980.050.330.05(0.G45)0.270.030.850.141(0. 14)(0.2)0.240.060.23 0.08(0.
7、1)In(0.02)QO37().O130.064 0.022(0.026)0.082 0.028(0.04)(0.02)(0.03)(0.06)La54422 + 256 + 521+262+41542.3+0.225 + 22.9+0.4LiI31518.3 0.99.5 0.911.1+0.54422034.8 1.024.7 2.411.22.3Lu1.15 0.09O.I2O.O3O.I9O.O50.30 0.030.41 0.050.140.030.023 0.0070.11 0.010.390.06Mn463+18604+18I3IO6I155+7173+11434 272844
8、30+141600 + 70Mo3.5 0.20.54 0.()92.6 0.20.76 0.140.35 0.09().38 0.()6().18 0.06(0.27)0.15 0.06N540 60(170)(68)Nb4036.8 1.46885.90.914.3+1.66.6 1.70.8 + 0.24.5 0.82.70.9Nd474I9254+421248312.01.01.960.142146.5 1.4Ni2.30.8I72140+716.61.137 + 3182(4)132117+10P405 201030 2441301229 7() 39690 342263157757
9、0 40360 20Pb31311.3+1.8小7.6+0.88.7+1.81835-27.6 2.0(8)岩石成分分析标准物质认定值与不确定度（续）质量夕擞 （10-6）花岗岩GBW07103 (GSR-1)安山岩GBW07104 (GSR-2)玄武岩GBW07105 (GSR-3)石英砂岩 GBW07106 (GSR-4)页岩GBW07107 (GSR-5)泥质灰岩 GBW07108 (GSR-6)石灰岩GBW07120(GSR-13)GBW07121(GSR-14)斜岫f人由GBW07122 (GSR-15)Pr12.70.84.9 0.4I3.2l.35.40.613.6l.73.4
10、0.40.60 0.145.80.81.250.15Rb466I738 + 3374292205 + 832+44.00.657529 + 5S380 3319221(100)860 42(66)(370)368(50)(60)Sb0.21+0.060.12 + 0.04(0.08)0.60+0.110.18 0.040. 43+0.110.072 + 0.0130.063+0.0130.63 + 0.25Sc6.1 0.49.5 0.7I5.2l.24.20.3I8.5l.26.0l.l(0.7)5.00.5434Se(0.04)(0.04)0.073 0.0240.08 0.030.075
11、 0.0150.09 0.020.021 0.0040.019 0.0070.083 0.009Sm9.7+0.83.4 0.210.2+0.54.70.38.4+ 0.42.4 0.20.40 0.053.3 + 0.32.1 0.2Sn12.5+1.5O.79O.I72.00.41.1 0.22.00.4(0.98)(0.5)0.8 + 0.2(0.8)Sr1(X)6790 35ll(X)6458590 791354107 9690 201429Ta7.20.70.400.104.30.60.38 0.050.90.10.42+0.05(0.05)(0.34)(0. I)Tb1.65+0.
12、090.41 0.051.2 0.20.79 0.091.02 0.080.35+0.050.054+0.0100.29+0.030.570.08Te().021 0.006().O17O.(X)5(0.022)().038 0.012(0.023)(0.024)Th54 + 32.6+0.36.0 0.87.0 0.412.8 + 0.94.1+0.50.86 0.071.9+0.2(0.4)Ti1720 7()3090 901420014001580 8()395() 13()196() 902 30 3()1800 140551() 160T11.93 0.38O.I6O.O5(0. 1
13、2)0.360.060.71 0.090. 33 0.07(0.03)(0.20)(0. 11)Tm1.06+0.09O.I5O.O50.280.040.320.040.43 0.030.17+0.04(0.024)0.11 0.020.370.i0u18.81.40.9() 0.191.4 0.32.1 0.31.5 0.31.9 0.30.24 0.04(0.4)(0. 14)V24 + 294 + 4167+113338743665.4+1.6454296 + 39w8.40.5(0.45)(0.4)1.2 0.20.790.140.67 0.180.13 0.030.38 + 0.09
14、0.34 0.09Y6259.3 1.22242I.52.226 + 29.1 1.61.9 0.47.30.92O3Yb7.4 0.50.89 + 0.131.5 0.41.9+0.22.60.30.90 + 0.110.15 0.050.69 0.082.4 0.4Zn2837I51501020255+452+47247310012ZrI6799911277 2021499696213ll3（100）(57)(IO-2)SiO：72.830.1060.62 0.1444.640.ll90.360.l559.230.l615.600.066.65 0.1466.270.2749.62 0.1
15、5AhCh13.40+0.0716.17+0.1213.83 0.133.520.09l8.820.145.03 + 0.080.68 0.0516.33 + 0.1513.76+0.19TFe2ch2.14 + 0.064.90 0.06I3.4OO.I93.22 + 0.077.60 + 0.092.52 + 0.070.21 0.013.12+0.0814.8+0.3FeO1.02 0.042.390.077.600.130.61 0.051.39 0.061.64 0.06(0.()6)(1.6)10.8 0.6MgO0.42 + 0.041.72+0.067.77 + 0.170.0
16、82 0.0202.01+0.055.19+0.120.71 0.091.63 + 0.107.2 + 0.3CaO1.55 0.055.2OO.O78.81 0.090.300.040.60 0.0435.670.255l.l0.42.660.109.6 + 0.2Na：O3.13 + 0.063.86 + 0.073.38O.O50.061 0.0140.35 0.02(0.08)0.03 0.015.3O.I2.07+0.09K：O5.01 0.071.89 0.052.32 0.060.65 0.034.160.100.780.040.15 0.022.60 0.060.48 0.05
17、HQO.6OO.O5(1.5)2.86 0.131.01 0.065.60.3(2. 12)(0.4)（1.0）(1.7)CO：(0. 15)3.47 + 0.07(0. 19)(0.19)(0. 10)32.4 + 0.339.8+0.30.35 + 0.05(0. 16)cor.(0.05)(0.16)(0. 11)(0.15)TC(0.10)(0.19)9.0 0.2LOI(0.70)4.44 0.12(2.24)1.100.07(5.95)34.1 0.240.2 0.4l.280.141.06 0.09说明：士 ”后的数据为不确定度,括号内的数值为参考值。质量分数 (10)GBVV0
18、7725GSR-16含铀砂岩GBW07726 GSR-17 二辉斜长麻粒岩GBW07727GSR-18 峨眉山玄武岩GBW07728GSR-19 辉石橄榄岩GBW07729 GSR-20 炭硅质页岩GBW07730GSR-21炭质硅质岩Ag0.046+0.0060.069+0.0070.085+0.0120.0860.0090. 18+0.020.24+0.03As4.7+0.40.490.081.80.20.840.141(). 10.66. 1+0.4B11.5+2.14.70.5(11)31.3+3.9Ba6051664916277949.21.6118535.93.7Be0.99+0.
19、071.370.091.99+0.090.28+0.031. 10+0.060. 13+0.02Bi0.061 0.0110.031 0.0070.0300.0150.270.020. 100.02Br(1.4)Cd0.071+0.0100.092+0.0070.0980.0160.0820.0043.20.2(0.035)Cc52.0+2.762.92.3104612.2 土 1.323.7 土 1.242.92.3Cl72.911.671.06.251.0+5.42442248.44.6Co7.6+0.721. 11.238.7+2.4149+124.90.42.30.4Cr27.73.4
20、96.76.098. 1+8.8(0.49*)1851620.6+3.6Cs1.80.2(0.28)0.520.081.40.22.20.20.43+0.08Cu4.90.633.5+1.7240875.64.740.9+2.98.6+1.3Dy4.9+0.43.7+0.38.9+0.61.20.12.50.30.88+0.08Er3.00.32.00.24.30.40.630.061.60.20.55+0.06Eu1.5+0.11.60.13.30.20.38+0.030.43+0.040. 17+0.03F278254242580137197+1954430(80)Ga10.60.32i.
21、51.025.00.94.90.56.8+0.6(1.6)Gd5.40.44.90.210.30.71.20.22.20.30.66+0.09Ge0.51 0.080.950.061.27+0.130.920.110.780.06Hf3.3 土 0.44.70.59.71.8(1.1)2.90.4(1.4)Hg*(9.9)(5)3.50.62202212.2+0.9Hol.060.ll0.750.081.660.160.230.030.540.070.18+0.03I0.37+0.051.03+0.11In0.025+0.0030.0490.0030. 104+0.0070.0230.0030
22、.0320.0020.015+0.004La30.02.529.41.248.02.45.80.613.20.93.50.5Li15.2+1.312. 1 0.6)1.30.65.90.312.61.00.59+0.05Lu0.400.050.30+0.040.51+0.050. 100.020.28+0.040. 120.02Mn0.21 0.01*816250. 14+0.01*0. 140.01*1411167l 1Mo0.33+0.060.640.081. 19+0.100. 19+0.0471.25.60.670.15N0.220.02*Nb(6)7.00.645. 1 2.55.5
23、0.86.90.7Nd26.61.533.40.86.40.611.41.22.90.2Ni13.5 12.815.544.8+1.469.72.112697777.43.38. 10.7P252210. 11 0.01*0. 19+0.01*2271366126(50)Pb12.31.47.40.96.21.0(3.3)10.20.815. 11.4Pr6.6+0.48.5 8.08.513.70.61.60.13. 1+030.87+0.06岩石成分分析标准物质认定值与不确定度(续)质量分数 (10)GBW07725 GSR-16 含铀砂岩GBW07726 GSR-17 二辉斜长麻粒岩GB
24、W07727 GSR-18 峨眉山玄武岩GBW07728 GSR-19 辉石橄榄岩GBW07729 GSR-20 炭硅质页岩GBW07730 GSR-21 炭质硅质岩Rb68.21.919.3 土 1.427. 11.26.91.032.0+1.5S(690)326 3144141159514+280.73* 0.640.76*(76)Sb0.0930.0110.0800.0160.230.030. 13+0.022.01 0.160.68().()6Sc6.70.616.70.926.61.410.60.95.4+0.52.4+0.3Se0.0400.0070.094+0.006(0.15)
25、0.20+0.0229.73.60.320.04Sm5.40.36. 10.211.60.61.32 1.291.582.30.20.760.13Sn1. l0.21.50.23.2+0.2(0.9)I.6+0.3(1)Sr252781823271 737.92.81563TaTb0.42 0.37、0.66 0.840.050.71+0.043.20.21.630.090.21 0.030.480.090.390.()40. 13+0.02TeTh3.70.4(0.02)(0.58)5.50.6(0.04)0.950.11(0.06)4. 10.61. 1+0.2Ti0. 17+0.01*0
26、.400.02*2.440.06*0.25+0.01*0.13+0.01*26416T10.430.050.10(0.06)(0.05)1.80+0.17(0.05)Tin0.430.060.320.040.580.070. 10+0.020.280.040. 11+0.02U68.04.6(0.25)1.56+0.100.320.0612.51.21.90.2V33.21.911553891870.37.46143128. 11.6W0.540.050. 150.030.540.05(0.17)0.700.100.530.05Y31. 11.017.8+0.737.51.65.90.916.
27、90.85.6+0.7Yb2.4+031.80.23.40.30.580.061.70.20.740.09Zn33.41.986.22.5142+1089.04.646.2+1.911.72.1Zr1148173113652139.24.8108553.35.4SiO2*46.40+0.3458.470.3747.950.1637.240.2171.51 0.2894.340.53A12O3*8.88+0.2117.140.2012.680.142.800.225.21+0.091.870.04TFeQ、*1.69 1.662.026.85+0.1413.760.2613.270.371.79
28、0.()40.66+0.04FcO* MgO*(0.5) 0.88().053.89+0.113.260.106. 160.135. 11+0.094.76+0.2532.260.702.620.08(0.05)CaO*20. 130.395.900.117.580.112. 17+0.064. 110.16(0.07)NaQ*K2O*1. 190.042.270.064.770.121.51+0.043.61+0.121. 19+0.020. 17+0.010.700.050.78+0.04(0.03)h2o*(2.5)2.790.20(8.6)(2)(0.7)CO2*cor*15.03+0.65(0.1)(0.1)(0.25)(1.3)0.340.035.250.194.82+0.301.560.()6TC*4.250.20(0.(0.1 1)(0.42)5.97 5.876.()51.67+0.04LOI*17.48+0.150.680.052.550.1610.340.2012.09().192.560.04注：“土”前为认定值，“土”后为不确定度；带括号数值为参考值，带号的数值为信息值；带 号的标准值为中位值，其下为置信限；带*号的数据含量单位为,带*号的数据含量单位 为 ng/g。